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1 H NMR (400 MHz, DMSO- d 6 ) δ 12.30 (s, 1H), 11.12 (s, 1H), 7.85–7.71 (m, 2H), 7.67–7.57 (m, 1H), 7.40 (d, J = 7.0 Hz, 1H), 6.77–6.66 (m, 1H), 5.12 (dd, J = 12.8, 5.4 Hz, 1H), 4.39 (d, J = 12.2 Hz, 1H), 4.05 (s, 2H), 3.91 (d, J = 13.7 Hz, 1H), 3.13 (t, J = 7.3 Hz, 2H), 3.03 (t, J = 12.0 Hz, 1H), 2.95–2.82 (m, 1H), 2.72 (dd, J = 21.2, 10.0 Hz, 1H), 2.57 (dd, J = 25.4, 13.1 Hz, 3H), 2.38–2.26 (m, 2H), 2.06 (dd, J = 10.7, 5.4 Hz, 1H), 1.81 (s, 2H), 1.67 (dd, J = 14.3, 7.2 Hz, 2H), 1.56–1.30 (m, 8H), 1.23–1.14 (m, 9H)

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